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The prevention of oxygen uptake during bottling

Charl Theron

The dissolved oxygen content in the bottle after bottling should ideally be less than 1 mg/l. Bearing in mind an uptake of 0.1 to 0.2 mg/l oxygen during the transfer of wine between tanks, it is obvious that the above-mentioned ideal scenario can only be achieved if the respective actions are executed with the greatest possible accuracy. All actions should be carefully monitored, because a few mistakes could spoil the entire operation.

If the bottling process is divided into the usual sequence of activities, the relevant actions to be initiated or applied may be summarised as follows:

Bottling tank

If bottling tanks are not filled to capacity, which is not supposed to happen, the space should be filled with inert gas. It will also be expedient to sparge inert gas through the wine even if the tanks are full. The use of argon or nitrogen as inert gases is recommended, in view of the fact that carbon dioxide is soluble in wine and may impart pétillance to the wine.

Wine hoses

The length of the hoses should be limited and any unnecessary coupling links avoided. Ensure that the hoses and coupling links are in good condition without any leakages. The hoses should prefereably be de-aerated with inert gas before the wine is racked.

Filter

Ensure that all filter connections have a tight seal and that air spaces are filled before wine is pumped through the filter.

Filling machine

Use vacuum filling machines if oxygen uptake during bottling has to be limited. Before the wine is pumped into the filling machine, oxygen pockets should be prevented by rinsing the filling machine with inert gas. The filling heights should be optimised and care taken that the desired filling heights are maintained in all bottles.

Pre-evacuation of the bottles

Bottles should be de-aerated with inert gas and a double evacuation of bottles with inert gas is even better.

Determination of oxygen in bottles

It is important to determine the oxygen levels in newly filled bottles to ensure that the preventative actions were successful.

Evacuation or rinsing of the filling space of bottles

Vacuum closure of bottles is beneficial provided its implementation is effective. The filling space should obviously be restricted to the minimum. Rinsing with inert gas apparently has limited advantages and the injection of liquid nitrogen is the most effective method.

Rinsing the closures

By rinsing the inside of hollow closures such as screw caps with inert gas before closure, oxygen uptake in the wine may be restricted.

Closed bottle

Once the bottling and closing processes have been completed, oxygen analyses of the wine and filling space should be conducted to determine the oxygen uptake.

Reference:

Crochiere, G.K. 2007. Practical Winemaking, January/February 2007: 74 - 84.

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